Measurement of uncertainty of catalpinoside in Ganmainingxin Capsule
LIU Jiyang1, WANG Xiaofei1, YU Ling1, YAO Hongwei1, HU Hao1, and CHAI Jiangping2
1. Institute for Drug Control of People’s Armed Police Force,Beijing 102613,China; 2. Guang Anmen Hospital,China Academy of Chinese Medical Sciences,Beijing 100053,China
Abstract:Objective To find out the effect factors of uncertainty by analyzing the uncertainty of measurement in determination of catalpinoside by HPLC and provide the evidence to evaluate the measurement. Methods The Catalpinoside in Ganmainingxin Capsules was determined by HPLC. The causes and effects were simplified and uncertainty was appraised. Results The uncertainty result was 2.70% and the result of content was(1.17±0.063)mg/g. Conclusions The mathematic model established is suitable for uncertainty analysis of catalpinoside by HPLC.
刘激扬,王晓飞,于玲,姚红伟,胡好,柴江平. 甘麦宁心胶囊中梓醇含量测定的不确定度分析[J]. 武警医学, 2015, 26(11): 1101-1104.
LIU Jiyang, WANG Xiaofei, YU Ling, YAO Hongwei, HU Hao, and CHAI Jiangping. Measurement of uncertainty of catalpinoside in Ganmainingxin Capsule. Med. J. Chin. Peop. Armed Poli. Forc., 2015, 26(11): 1101-1104.